dimy_grass

At 60 C, (A48) became a mush of crystals. Added 27 g H2O. Temp dropped
to 54 C. Reheated to 60 C to dissolve all. On cooling saturated again
at 57 C, crystallized at 55 C.

Added more water to total wt 135 g. Dissolved all at 38 C. Decanted at 29.5 C:

* Solid (A50) needle-like crystals, tangled, 23.4 g.

* Liquid (A51) very light yellow clear, 150 g. Merged with (A29) into
(A19).

Put (A29) in cooling bath when it was 26 C. Started to crystallize at
7.5 C, more at 7,4 C. Decanted:

* Liquid (A52) clear light yellow, 352 g.

* Solid (A53) fine crystals, 9 g. Tried to wash with ethanol 92% but
collapsed and continued wet.

In test tube (E6) placed 4 mL of (A47)+(A45) and 8 mL ethanol 46%.
Became slightly cloudy. By 2017-03-01 had deposited a light fluffy
white ppt.

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